

Available forms:clear colourless to very slightly brown liquid
pd_proNo:481376-2fb25157-3726-4f6c-bc5a-cb3e767d5bae
pd_productuse:
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Synthesis Reference(s) |
Chemical and Pharmaceutical Bulletin, 34, p. 486, 1986 DOI: 10.1248/cpb.34.486Synthesis, p. 1091, 1982 DOI: 10.1055/s-1982-30083 |
|
Purification Methods |
Shake it with lead peroxide, filter and distil it in a vacuum under N2. [Beilstein 1 IV 1560.] |
InChI:InChI=1/C8H18S2/c1-3-5-7-9-10-8-6-4-2/h3-8H2,1-2H3
Thiolates are a widely used ligand class...
The catalytic activity of the tetrapyraz...
1. A study was made of the reaction of n...
The synergistic effect of a Lewis acid (...
Development of visible-light-induced pho...
Temperature-and solvent-induced selectiv...
Recently, inexpensive and readily availa...
α,α-bis(butylthio)toluene
dibutyl disulfide
benzaldehyde
| Conditions | Yield |
|---|---|
|
With
water; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate;
In
tetrahydrofuran; dichloromethane;
at 23 ℃;
Mechanism;
other acyclic dithioacetal (R=Ph);
|
80% |
n-butanethiol
2-Methyl-dithiopropionsaeure-phenylester
dibutyl disulfide
thiophenol
2-Methyl-dithiopropionsaeure-butylester
diphenyldisulfane
| Conditions | Yield |
|---|---|
|
With
di-tert-butyl peroxide;
In
benzene;
at 140 ℃;
for 8h;
Further byproducts given. Yields of byproduct given;
|
1.1 g |
1-bromo-butane
tetrachloromethane
sodium 1-buthanethiolate
vinyl acetate
1,2-bis-butylsulfanyl-1-phenyl-ethane
butyl methyl disulfide
4-butyldisulfanyl-3-nitro-benzoic acid
n-butyl methyl sulfide
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